Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the. ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Copper – Copper Sulfate – 16% sulfuric acid, ASTM A – Practice E (Strauss Test). ASTM A Practice E test. This practice describes the procedure by which the copper-copper sulfate% sulfuric acid test is conducted to determine .
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Because it can be run quickly for screening, we often run this test first. Pracice structure sensitization was observed in test sample after etched under high optical microscope.
The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. For example, many low-carbon and stabilized stainless steels e. It is not sensitive to size or orientation, provided that edge attack is not ignored. Bend Specimen after soaking. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.
The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes. However, when a material is exposed to asgm temperatures for long periods of time, a process called sensitization may occur. Strauss practide specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours.
The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:. Test sample was etched using Oxalic Acid with electrolyte etching. Examination of intergranular cracks and fissures on bend surface.
Corrosion Tests are conducted to determine the resistance of a metal to chemical attack. What is your typical turnaround time? Historical Version s – view previous versions of standard. Please refer to the specification for more details. For example, in highly oxidizing solutions, intergranular attack can occur due to prqctice phases, while attack of carbides may occur somewhat less oxidizing solutions.
ASTM A Intergranular Corrosion Testing and Analysis
Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.
Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. The etch structure types used to classify the specimens are: The inch-pound equivalents are in parentheses and may be approximate. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.
The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels.
The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack. This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means.
Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.
The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use. The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack.
Intergranular Corrosion Testing: An Overview of ASTM A262
Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.
This test method describes the procedure for conducting the ferric chloride corrosion test for detecting the presence of detrimental intermetallic phases in Duplex Stainless Steels. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.
Learn more about our laboratories – where astk are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack.
At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific pracyice type.
Edges shall be rounded and a fine final polish is required at all surface exclude the weld cap and root area. Corrosion is measured by a weight loss that is converted to a corrosion rate. Sample condition astk soaking in Ferric chloride solution.
This test method does not determine the critical pitting temperature or test for the suitability for use in a particular environment. This method is a hour boiling test for “as received” specimens of stainless steel. News Project Details Tools. Discover perspectives, resources, and advice from our world-leading Engaged Experts.
Please share this page: See Appendix X1 for information regarding test selection. Intergranular cracking or crazing is evidence of susceptibility.
ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results. These practices include five intergranular corrosion tests, namely: This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. How do you select the right ASTM corrosion testing method for your material?
It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. A bend test followed by a visual or micro-examination are used pracctice determine “Pass” or “Fail” of test specimens. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract practoce accurate, complete or up to date.